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MI 2335-2003

МИ 2335-2003

State system for ensuring uniformity of measurements. Internal quality control of quantitative chemical analysis results

Государственная система обеспечения единства измерений. Внутренний контроль качества результатов количественного химического анализа

Status: Not effective. The use of MI 2335-2003 in the Russian Federation was discontinued due to the introduction of RMG 76-2004 "State system for ensuring the uniformity of measurements. Internal quality control of the results of quantitative chemical analysis" (according to information from the document developer - FSUE UNIIM). At the same time, MI 2335-2003 is included in all Indexes of "Normative documents in the field of metrology" (effective in the Russian Federation since 2010 and subsequent years)

This recommendation establishes the order and content of work on the internal (internal) quality control of the results of quantitative chemical analysis in the implementation in a separate laboratory of a specific methodology with established quality indicators.

Настоящая рекомендация устанавливает порядок и содержание работ по внутрилабораторному (внутреннему) контролю качества результатов количественного химического анализа при реализации в отдельной лаборатории конкретной методики с установленными показателями качества.

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Format: Electronic (pdf/doc)

Approved: FSUE UNIIM, 9/30/2003

SKU: RUSS154005

Price: $953.00



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The Product is Contained in the Following Classifiers:

Construction (Max) » Regulations » Regulatory documents of supervisory authorities » Normative documents of Committee of Russian Federation for Standardization, Metrology and Certification »

PromExpert » SECTION II. METROLOGICAL » I Organizational and technical bases of metrological support » 1 Organization and management of metrological support » 1.2 Organization of activities of metrological services »

ISO classifier » 17 METROLOGY AND MEASUREMENTS. PHYSICAL PHENOMENA » 17.020 Metrology and measurements in general »


The Document References:

GOST 8.315-97: Standard samples for composition and properties of substances and materials

GOST R 1.12-99: State system for standardization of Russian Federation. Standardization and related activities. Terms and definitions

GOST R 50779.40-96: Statistical methods. Control charts. General guide and introduction

GOST R 50779.42-99: Statistical methods. Shewhart control charts

GOST R 50779.71-99: Statistical methods. Sampling procedures for inspection by attributes. Part 1. Sampling plans indexed by acceptable quality level (AQL) for lot-by-lot inspection

GOST R 8.563-96: State system for ensuring the uniformity of measurements. Procedures of measurements

GOST R ISO 5725-1-2002: Accuracy (trueness and precision) of measurement methods and results. Part 1. General principles and definitions

GOST R ISO 5725-2-2002: Accuracy (trueness and precision) of measurement methods and results. Part 2. Basic method for the determination of repeatability and reproducibility of a standard measurement method

GOST R ISO 5725-3-2002: Accuracy (trueness and precision) of measurement methods and results. Part 3. Intermediate measures of the precision of a standard measurement method

GOST R ISO 5725-4-2002: Accuracy (trueness and precision) of measurement methods and results. Part 4. Basic methods for the determination of the trueness of a standard measurement method

GOST R ISO 5725-6-2002: Accuracy (trueness and precision) of measurement methods and results. Part 6. Use in practice of accuracy values

GOST R ISO/IEC 17025-2000: General requirements for the competence of testing and calibration laboratories

MI 2334-2002: State system for ensuring uniformity of measurements. Certified mixtures. General development requirements

MI 2336-2002: State system for ensuring uniformity of measurements. Indicators of accuracy, accuracy, precision of methods for quantitative chemical analysis. Assessment methods

The Document is Referenced By:

GOST 15483.10-2004: Tin. Methods of atomic-emission spectral analysis

GOST R 51232-98: Drinking water. General requirements for organization and quality control methods

GOST R 51755-2001: Silicate enamels (frits). Methods of analysis

GOST R 52599-2006: Precious metals and their alloys. General requirements for methods of analysis

GOST R 53403-2009: Iron ores, concentrates, agglomerates and pellets. Method for the determination of titanium content

GOST R 53657-2009: Iron ores, concentrates, agglomerates and pellets. Method for determination of divalent iron calculated as ferrous oxide

GOST R 53658-2009: Iron ores, concentrates, agglomerates and pellets. Atomic absorption method for determination of copper content

GOST R 53659-2009: Iron ores, concentrates, agglomerates and pellets. Atomic absorption method for determination of total manganese calculated as protoxide

GOST R 54922-2012: Zink concentrates. Technical specification

GOST R 8.613-2005: State system for ensuring the uniformity of measurements. Procedures for quantitative chemical analysis of water samples. General requirements for development

MI 1936.01-2000: Method for determining the mass concentration of total mercury by atomic absorption

MI 2240-98: National Measurement Standards. Analysis of Measurement, Inspection, and Testing Practicies at Businesses, Organizations, and Associations. Work Execution Technique and Procedures

MI 2334-2002: State system for ensuring uniformity of measurements. Certified mixtures. General development requirements

MI 2422-97: State system for ensuring uniformity of measurements. Gas analyzer in solid materials "Eltra ONH". Method of verification

MI 2500-98: National Measurement Standards. Basic Principles for Metrological Assurance for Small Businesses

MI 2600-2000: Recommendation. State system for ensuring uniformity of measurements. Checking the suitability for use in the laboratory of reagents with expired shelf life according to the results of internal laboratory control of measurement accuracy

MI 2612-2000: State system for ensuring uniformity of measurements. Metrological criteria for assessing the conformity of the quality of the certification object to regulatory requirements

MI 2878-2004: State system for ensuring uniformity of measurements. Mass concentration of total mercury in the soil. Measurement Technique by Atomic Absorption

MI 2881-2004: Recommendation. GSE. Methods of quantitative chemical analysis. Procedures for testing the acceptability of analysis

MI 2976-2006: Recommendation. State system for ensuring uniformity of measurements. Construction, content and presentation of documents governing the methods of quantitative chemical analysis

MU 08-47/074: Quantitative chemical analysis of samples of biological objects (blood, urine). Method for measuring mass concentrations of mercury by inversion voltammetry

MU 08-47/077: Quantitative chemical analysis of food samples (fatty foods). Methodology for measuring mass concentrations of arsenic and iron by inversion voltammetry

MU 08-47/082: Methods for the quantitative chemical analysis of samples of drinking, mineral, natural and treated wastewater for the content of selenium by inversion voltammetry

MU 08-47/084: Methods for the quantitative chemical analysis of samples of oral hygiene products for the content of zinc, cadmium, lead, copper and mercury by inversion voltammetry

MU 08-47/088: Vitaminized feed and top dressing. Determination of mass concentrations of vitamin B2 by differential voltammetry

MU 08-47/136: Food products and food raw materials. Inversion voltammetric methods for determining the content of toxic elements (cadmium, lead, copper and zinc)

MU 08-47/138: Flour, cereals, bread, bakery and flour and cereal products. Voltammetric method for measuring the mass concentration of mercury

MU 08-47/141: Biologically active additives. Voltammetric method for determining the mass concentrations of vitamins C, B1, B2, E and quercetin

MU 08-47/156: Alcoholic drinks. Inversion voltammetric method for measuring the mass concentration of nickel

MU 08-47/157: Milk and dairy products. Inversion voltammetric method for measuring the mass concentration of cobalt

MU 08-47/160: Milk and dairy products. Inversion voltammetric method for measuring the mass concentration of mercury

MU 08-47/162: Natural, drinking and treated sewage. Voltammetric method for measuring the mass concentration of mercury

MU 08-47/166: Alcoholic extracts and tinctures of medicinal herbs, fruits and berries. Voltammetric method for determination of mass concentrations of quercetin and rutin

MU 08-47/167: Fish, seafood, non-fish fishing objects and products produced from them. Voltammetric method for measuring the mass concentration of mercury

MU 08-47/177: Biologically active additives. Inversion voltammetric method for determining the mass concentration of iodine

MU 08-47/189: Natural, drinking, technologically clean, purified waste water. Voltamperometric method for measuring phenol mass concentrations

MU 08-47/196: Meat and meat products. Inversion voltammetric method for measuring the mass concentration of mercury

MU 08-47/204: Flour, groats, flour-and-cereals, bread and bakery products with additives of vitamin-mineral mixtures. Voltammetric method for measuring the mass concentration of vitamin B1

MU 08-47/205: Medications. Voltammetric method for measuring the mass fraction of azithromycin dihydrate

MU 08-47/206: Food products and food raw materials. Voltammetric method for measuring the mass concentration of iodine

MU 08-47/215: Grape, fruit wines and wine materials. Method for measuring mass concentration of citric acid by potentiometric titration

MU 08-47/218: Hair. Method for measuring mass concentration of calcium by amperometric titration

MU 2.6.1.26-2000: Dosimetric control of occupational internal exposure. General requirements

MUK 4.1.1221-03: Measurement of concentrations of clethodim and its main metabolites (clethodim sulfone and clethodim sulfoxide) in the air of the working area using high performance liquid chromatography

MUK 4.1.1222-03: Measurements of clomazone concentrations in leafy and sugar beet roots, carrots and potato tubers by gas-liquid chromatography (addition to МУ 5006-89)

MUK 4.1.1223-03: Determination of residual amounts of metribuzin in potato tubers by gas-liquid chromatography

MUK 4.1.1225-03: Measurement of metsulfuron-methyl concentrations in the air of the working area and ambient air of populated areas using high performance liquid chromatography

MUK 4.1.1227-03: Measurement of nicosulfuron concentrations in the working area air by high performance liquid chromatography

MUK 4.1.1229-03: Determination of residual amounts of tetraconazole in water, soil, green mass, grain and straw of grain crops by gas chromatography

MUK 4.1.1231-03: Measurement of the concentration of Tralkoxydim in the air of the working area by high performance liquid chromatography

MUK 4.1.1232-03: Determination of residual amounts of trifloxystrobin in water, soil, apples and its metabolite TsGA 321113 in water and soil by gas chromatography

MUK 4.1.1233-03: Measurement of concentrations of trifloksistrobina in the air of the working area and atmospheric air by gas chromatography

MUK 4.1.1236-03: Determination of residues of flufensin in water, soil, apples, grapes, grape and apple juice by chromatographic methods

MUK 4.1.1405-03: Determination of residual amounts of metribuzin in water, soil, potato tubers, tomato fruits, corn grain, seeds and soybean oil by gas chromatography

MUK 4.1.1406-03: Measurement of abamectin concentrations by high performance liquid chromatography in the air of the working area

MUK 4.1.1407-03: Measured concentrations of Buprofezin in working zone air by gas-liquid chromatography

MUK 4.1.1412-03: Measurement of carboxin concentrations in the air of the working area and in the atmospheric air of populated areas using high performance liquid chromatography

MUK 4.1.1413-03: Measurement of clefoxim concentration in the air of the working area by high performance liquid chromatography

MUK 4.1.1414-03: Measurement of clomazone concentrations in the air of the working area using high performance liquid and gas-liquid chromatography

MUK 4.1.1415-03: Determination of clomazone in water by chromatographic methods

MUK 4.1.1419-03: Measurement of phenmedipham concentrations in the atmospheric air of populated areas using high performance liquid chromatography

MUK 4.1.1420-03: Measurement of fludioxonil concentrations in the working area air by high performance liquid chromatography

MUK 4.1.1451-03: Determination of residual amounts of ammonium glufosinate and its metabolite in water, seeds and sunflower oil by gas chromatography

MUK 4.1.1461-03: Determination of residual amounts of fenoxaprop-P and fenoxaprop-P-ethyl in water and fenoxaprop-P in soil, grain and straw of cereal crops, green mass, seeds and oil of sunflower, flax, soybeans and rapeseed, green leaves, sugar crops and root crops and

MUK 4.1.1473-03: Guidelines for the determination of residual quantities of desmedipham and phenmedipham in root crops and tops of sugar, table and fodder beet by capillary gas-liquid chromatography

MUK 4.1.1476-03: Guidelines for the determination of residual amounts of pendimethalin in water, soil, cabbages, seeds and oil of sunflower by gas-liquid chromatography

MUK 4.1.1804-03: Guidelines for the determination of residual amounts of pro-sulfuron in water, soil, grain and straw of cereal crops, green mass and corn grain, flax seeds by high performance liquid chromatography

MUK 4.1.1805-03: Guidelines for the determination of residual amounts of thiamethoxam in cabbage, green mass, seeds and oil of rapeseed and mustard, currant by high performance liquid chromatography

MUK 4.1.1806-03: Guidelines for the determination of residual amounts of chlorsulfuron in water, soil, grain and straw of cereal crops, seeds and straw of flax by high performance liquid chromatography

MUK 4.1.1814-03: Methodical instructions for determining residual amounts of fluazinam in water, soil, potatoes using gas chromatography

MUK 4.1.1815-03: Guidelines for determining residual amounts of hozalofop-p-ethyl in water, soil, potato tubers, root crops and tops of sugar, table beet and fodder beet, seeds and soybean oil, seeds and straw of flax in the main metabolite hizalofop-p acid with using cap

MUK 4.1.1834-04: Guidelines for the determination of residual amounts of tebuconazole in seeds and sunflower oil by gas-liquid chromatography

MUK 4.1.1836-04: Guidelines for the determination of residues of pyriproxifene in green mass, cucumbers and tomatoes by high performance liquid chromatography

MUK 4.1.1850-04: Guidelines for the determination of residues of acetamiprid in water, soil, tops and potato tubers, grain and straw of cereal crops

MUK 4.1.1906-04: Guidelines for the determination of residual amounts of spiroxamine in rice grains and straw by gas-liquid chromatography

MUK 4.1.1942-05: Methodical instructions for determining residual amounts of haloxyfop-P-methyl in onion turnips by capillary gas-liquid chromatography

MUK 4.1.1943-05: Guidelines for the determination of residual quantities of deltamethrin in green mass, seeds and rapeseed oil by gas chromatography

MUK 4.1.1947-05: Methodical instructions for determining residual quantities of diflubenzuron in apples by high performance liquid chromatography

MUK 4.1.1949-05: Guidelines for determining residual amounts of imidacloprid in green mass, grain and straw of cereal crops, green mass, seeds and rapeseed oil by high performance liquid chromatography

MUK 4.1.1953-05: Guidelines for determining residual amounts of hizalofop-P-ethyl in onion turnips, carrot roots and cabbages for the main metabolite of hizalofop-P acid by capillary gas-liquid chromatography

MUK 4.1.1965-05: Determination of residual amounts of flutriafol in apple fruits, berries and grape juice by gas-liquid chromatography

MUK 4.1.1967-05: Determination of residues of kresoxim-methyl in cucumbers, tomatoes, berries and grape juice by gas chromatography

MUK 4.1.1969-05: Determination of residual amounts of acetochlor in bottova, sugar beet roots and carrot roots by gas-liquid chromatography

MUK 4.1.1972-05: Determination of residual amounts of metribuzin in water, soil, tomatoes and potatoes by gas-liquid chromatography

MUK 4.1.1978-05: Determination of glyphosate residues in soybean grain and oil, seeds and sunflower oil by high performance liquid chromatography

MUK 4.1.2103-06: Determination of the mass concentration of vanadium in blood samples by atomic absorption spectrometry with electrothermal atomization

MUK 4.1.2104-06: Determination of the mass concentration of copper, magnesium, cadmium in urine samples by atomic absorption spectrometry

MUK 4.1.2105-06: Determination of the mass concentration of manganese, lead, magnesium in hair samples by atomic absorption spectrometry

MUK 4.1.2106-06: Determination of the mass concentration of manganese, lead, magnesium in blood samples by atomic absorption spectrometry

MUK 4.1.2107-06: Determination of the mass concentration of phenol in biological media (urine) by gas chromatography

MUK 4.1.2108-06: Determination of the mass concentration of phenol in biological media (blood) by gas chromatography

MUK 4.1.2109-06: Determination of the mass concentration of 2-chlorophenol in biological media (urine) by gas chromatography

MUK 4.1.2110-06: Determination of the mass concentration of formaldehyde, acetaldehyde, propionic aldehyde, butyraldehyde and acetone in urine samples by high performance liquid chromatography

MUK 4.1.2111-06: Measurement of mass concentration of formaldehyde, acetaldehyde, propionic aldehyde, butyraldehyde and acetone in blood samples using high performance liquid chromatography

MUK 4.1.2112-06: Determination of the mass concentration of chloroform, 1, 2-dichloroethane, carbon tetrachloride, chlorobenzene in biological media (blood) by gas chromatography

MUK 4.1.2113-06: Determination of the mass concentration of chloroform, 1, 2-dichloroethane, carbon tetrachloride in biological media (urine) by gas chromatographic analysis of an equilibrium vapor

MUK 4.1.2114-06: Determination of the mass concentration of chloroform, 1, 2-dichloroethane, carbon tetrachloride, chlorobenzene in biological media (urine) by gas chromatography

MUK 4.1.2115-06: Determination of the mass concentration of chloroform, 1, 2-dichloroethane, carbon tetrachloride in biological media (blood) by gas chromatographic analysis of an equilibrium vapor

MUK 4.1.2116-06: Determination of the mass concentration of styrene in blood samples by high performance liquid chromatography

MUK 4.1.2228-07: Chromato-mass-spectrometric determination of the sum of steroid saponins Yuss Schidiger in water

MUK 4.1.2283-07: Measurement of the concentration of metaldehyde in the atmospheric air of populated areas using gas-liquid chromatography

MUK 4.1.2291-07: Measurement of naphthalic anhydride concentrations in ambient air of populated areas using high performance liquid chromatography

MUK 4.1.2333-08: Measurement of diquat concentrations in the atmospheric air of populated areas using high performance liquid chromatography

MUK 4.1.3056-13: Measurement of mass concentrations of vinyl chloride and 1, 2-dichloroethane in blood samples by gas chromatographic analysis of an equilibrium vapor

MUK 4.1.3057-13: Measurement of the mass concentration of chloroethanol in blood samples by capillary gas chromatography

MUK 4.1.3230-14: Measurement of mass concentrations of chemical elements in biological media (blood, urine) using mass spectrometry with inductively coupled plasma

MUK 4.1.3231-14: Measurement of mass concentrations of N-nitrosoamines (N-nitrosodimethylamine, N-nitrosodiethylamine) in urine using capillary gas chromatography

MUK 4.1.3232-14: Measurement of the mass concentration of acrolein in the urine by high performance liquid chromatography

MUK 4.1.3233-14: Measurement of mass concentrations of 2, 4-dichlorophenol and 2, 4, 6-trichlorophenol in the blood by capillary gas chromatography

MUK 4.1.3474-17: Measurement of mass concentration of thiodiglycolic acid in urine by capillary gas-liquid chromatography

MUK 4.1.3475-17: Measurement of mass concentration of thiodioacetic acid in urine by gas chromatography-mass spectrometry

MUK 4.1.3476-17: Measurement of mass concentration of fluoride ions in hair samples by potentiometric method using an ion-selective electrode

MUK 4.1.3477-17: Measurement of the mass concentration of monochloracetic acid in urine samples by capillary gas chromatography

MUK 4.1.3478-17: Measurement of the content of volatile N-nitrosoamines (N-nitrosodimethylamine, N-nitrosodiethylamine) in dairy products (cereals for children) by chromato-mass spectrometric method

MUK 4.1.3479-17: Measurement of mass concentrations of N-nitrosoamines (N-nitrosodimethylamine, N-nitrosodiethylamine) in blood by capillary gas chromatography

MUK 4.1.3480-17: Measurement of mass concentrations of chemical elements (cadmium, lead, arsenic, mercury) in milk and dairy products by inductively coupled plasma mass spectrometry

MUK 4.1.3481-17: Measurement of mass concentrations of chemical elements in atmospheric air by inductively coupled plasma mass spectrometry

MUK 4.1.3482-17: Measurement of the mass concentration of vitamin K1 in serum by high performance liquid chromatography (HPLC)

MUK 4.1.769-99: Quantitative determination of formaldehyde in the urine by high performance liquid chromatography

MUK 4.1.770-99: Quantitative determination of formaldehyde in blood by high-performance liquid chromatography

MUK 4.1.771-99: Gas chromatography determination of concentrations of methyl, ethyl, isopropyl, propyl, isobutyl and butyl alcohols in urine

MUK 4.1.772-99: Gas chromatographic determination of concentrations of methyl, ethyl, isopropyl, propyl, isobutyl and butyl alcohols in the blood

MUK 4.1.773-99: Quantitative determination of fluoride ions in urine using an ion-selective electrode

MUK 4.1.994-00: Sanitary-chemical assessment of polymeric materials intended for use in video display terminals, personal electronic computers and elements of systems based on them

MVI.MN 3008-2008: Method for determining the mass fraction of pantothenic acid in specialized foods and dietary supplements

MVI.MN 3491-2010: Methods for measuring the content of chlorides in specialized products for baby food

ODM 218.9.010-2016: Guidelines for the automation of laboratory control

OST 41-08-214-04: Industry standard. Quality management of analytical work. Internal laboratory control of the accuracy (accuracy and precision) of the results of quantitative chemical analysis

OST 41-08-272-04: Quality control of analytical work. Geological control quality methods of analytical work.

PND F 12.10.1-2000: Guidelines for verifying the quality of chemical reagents used in performing quantitative chemical analysis.

PR 50.2.013-97: GSOEI. The procedure for accreditation of the metrological services of legal entities to the right of certification of measurement procedures and metrological examination of documents

R 50.2.008-2001: National System for Standardization of Measurements. Techniques for Chemical Quantitative Analysis. Scope and Procedure for Execution of Metrological Expert Review

R 52.24.309-2004: Organizing and secure monitoring of surface water pollution on Federal Hydrometereology and Environmental Monitoring Service web

RD 153-34.0-04.202-98: Procedural Guidelines. Certification of Departments of Energy Facilities Performing Quantitative Chemical Analysis. Organization and Procedure

RD 153-34.2-21.544-2002: Guidelines for the chemical control of corrosion processes in water filtration through concrete and reinforced concrete hydraulic structures

RD 52.10.728-2010: Basic requirements for the competence of laboratories in monitoring the status and pollution of sea water. State Oceanographic Institute (GOIN)

RD 52.18.180-2001: Guidelines. Determination of the mass fraction of organic halide pesticides n, n.-DDT, n, n "- DDE, alpha-HCH, gamma-HCH, trifluralin in soil samples. Methodology for measurement using gas-liquid chromatography

RD 52.18.180-2011: Guidelines. Determination of the mass fraction of organic halide pesticides P, P-DDT, P, P-DDE, alpha-HCH, gamma-HCH, trifluralin in soil samples. Methodology for measurement using gas-liquid chromatography

RD 52.18.310-2011: Mass fraction of organophosphorus pesticides parathion-methyl, fosalone, dimethoate in soil samples. Method of measurement by gas-liquid chromatography

RD 52.18.571-2011: Method for measuring the mass fraction of arsenic in soil and sediment samples using atomic absorption spectrometry with electrothermal atomization. NGO "Typhoon"

RD 52.18.583-2011: Method for measuring the mass fraction of antimony in samples of soils and bottom sediments by atomic absorption spectrometry with electrothermal atomization. NGO "Typhoon"

RD 52.18.623-2011: Mass fraction of herbicides bentiocarb and molinate and the identification of propanil and its metabolite 3, 4-dichloraniline in soil samples. Method of measurement by gas-liquid chromatography

RD 52.18.647-2003: Guidelines. Determination of the mass fraction of petroleum products in soils. Gravimetric Measurement Technique

RD 52.18.656-2011: Mass fraction of synthetic pyrethroids deltamethrin, fenvalerate, alpha-cypermethrin in soil samples. Method of measurement by gas-liquid chromatography

RD 52.18.685-2006: Guidelines. Determination of the mass fraction of metals in soil samples and bottom sediments. The method of measurement using atomic absorption spectrophotometry. NGO "Typhoon"

RD 52.18.718-2008: Organization and procedure for the observation of soil pollution by toxicants of industrial origin

RD 52.24.309-2011: Organization and conduct of regime monitoring of the state and pollution of surface land waters

RD 52.24.509-2005: Internal hydro-chemical information quality control

RD 52.24.609-2013: Organizing and conducting observations on the content of pollutants in bottom sediments of water bodies

RMG 76-2004: State system for ensuring the uniformity of measurements. Internal control of quantitative chemical analysis result's accuracy

RMG 94-2009: State system for ensuring the uniformity of measurements. Test laboratories performing of the quality control of oil at acceptance operations. Basic requirements

SDA 15-2009: Requirements to testings laboratories

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