MI 2881-2004
МИ 2881-2004
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Recommendation. GSE. Methods of quantitative chemical analysis. Procedures for testing the acceptability of analysis
Рекомендация. ГСИ. Методики количественного химического анализа. Процедуры проверки приемлемости результатов анализа
Status: Effective - Introduced for the first time
The recommendation applies to methods of quantitative chemical analysis, certified in accordance with GOST R 8.563 with the established values of repeatability and reproducibility indicators, and contains procedures for checking the acceptability of: results of a single analysis (parallel definitions) of working samples obtained under repeatability conditions; results of analysis of working samples obtained in reproducible conditions.
Рекомендация распространяется на методики количественного химического анализа, аттестованные в соответствии с ГОСТ Р 8.563 с установленными значениями показателей повторяемости и воспроизводимости, и содержит процедуры проверки приемлемости: результатов единичного анализа (параллельных определений) рабочих проб, получаемых в условиях повторяемости; результатов анализа рабочих проб, получаемых в условиях воспроизводимости.
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Format: Electronic (pdf/doc)
Approved: FSUE UNIIM,
6/20/2004
SKU: RUSS154291
The Product is Contained in the Following Classifiers:
PromExpert »
SECTION II. METROLOGICAL »
I Organizational and technical bases of metrological support »
1 Organization and management of metrological support »
1.2 Organization of activities of metrological services »
PromExpert »
SECTION I. TECHNICAL REGULATION »
V Testing and control »
3 Activities of testing laboratories »
3.1 Basic requirements for testing laboratories and their activities »
ISO classifier »
17 METROLOGY AND MEASUREMENTS. PHYSICAL PHENOMENA »
17.020 Metrology and measurements in general »
The Document References:
GOST R 8.563-96: State system for ensuring the uniformity of measurements. Procedures of measurements
GOST R ISO 5725-1-2002: Accuracy (trueness and precision) of measurement methods and results. Part 1. General principles and definitions
GOST R ISO 5725-6-2002: Accuracy (trueness and precision) of measurement methods and results. Part 6. Use in practice of accuracy values
MI 2335-2003: State system for ensuring uniformity of measurements. Internal quality control of quantitative chemical analysis results
MI 2336-2002: State system for ensuring uniformity of measurements. Indicators of accuracy, accuracy, precision of methods for quantitative chemical analysis. Assessment methods
The Document is Referenced By:
FR 1.31.2016.24509: Quantitative chemical analysis of water. Method for measuring the mass concentration of ethylene glycol and diethylene glycol in samples of natural and waste water by gas chromatography
FR 1.31.2018.30110: Quantitative chemical analysis of water. Method for measuring the pH of water samples by potentiometric method
GOST 18309-2014: Water. Methods for determining phosphorous substances
GOST 31857-2012: Drinking water. Methods for determination of surfactants content
GOST 31858-2012: Drinking water. Method for determination of chlorine-organic pesticides by gas-liquid chromatography
GOST 31868-2012: Water. Methods for determination of colour
GOST 31870-2012: Drinking water. Determination of elements content by atomic spectrometry methods
GOST 31940-2012: Drinking water. Methods for determination of sulfate content
GOST 31940-2013: Drink water Methods for determining sulphates content
GOST 31941-2012: Drinking water. Methods for determination of 2.4-D
GOST 31951-2012: Drinking water. Determination of volatile halogenated organic compounds by gas chromatography
GOST 31954-2012: Drinking water. Methods of hardness determination
GOST 31957-2012: Water. Methods for determination of alkalinity and mass concentration of carbonates and hydrocarbonates
GOST 31958-2012: Water. Methods for determination of total and dissolved organic carbon
GOST 33045-2014: Water. Methods for determination of nitrogen-containing matters
GOST R 52991-2008: Water. Methods for determination of total and dissolved organic carbon
GOST R 53403-2009: Iron ores, concentrates, agglomerates and pellets. Method for the determination of titanium content
GOST R 53657-2009: Iron ores, concentrates, agglomerates and pellets. Method for determination of divalent iron calculated as ferrous oxide
GOST R 53658-2009: Iron ores, concentrates, agglomerates and pellets. Atomic absorption method for determination of copper content
GOST R 53659-2009: Iron ores, concentrates, agglomerates and pellets. Atomic absorption method for determination of total manganese calculated as protoxide
GOST R 56157-2014: Soil. Procedures (methods) of analysis of composition and properties of soil samples. General requirements for development
GOST R 8.613-2013: State system for ensuring the uniformity of measurements. The procedures (methods) of measurements of structure and properties of water samples. General requirements to development
MI 2976-2006: Recommendation. State system for ensuring uniformity of measurements. Construction, content and presentation of documents governing the methods of quantitative chemical analysis
MUK 4.1.013-18: Method for measuring the mass fraction of 4-aminobenzoic acid in soil samples by the photometric method
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MUK 4.1.022-18: Methods of measuring the mass concentration of 2- (2,4-dinitrophenoxy) ethanol in water samples from water bodies of drinking and cultural and domestic water use by high performance liquid chromatography
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MUK 4.1.024-18: Methods for measuring the mass concentration of triethyl-O-acetyl citrate in the atmospheric air of populated areas using gas chromatography
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MUK 4.1.026-18: The method of measuring the mass concentration of triethyl-O-acetyl citrate in water samples of water bodies of drinking, cultural and domestic water use by gas chromatography
MUK 4.1.027-18: Method for measuring the mass fraction of triethyl-O-acetyl citrate in soil samples by gas chromatography
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MUK 4.1.031-18: Method for measuring the mass fraction of the main lead-nickel salt of phthalic acid in soil samples by high-performance ion-exchange chromatography
MUK 4.1.3057-13: Measurement of the mass concentration of chloroethanol in blood samples by capillary gas chromatography
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MUK 4.1.3474-17: Measurement of mass concentration of thiodiglycolic acid in urine by capillary gas-liquid chromatography
MUK 4.1.3476-17: Measurement of mass concentration of fluoride ions in hair samples by potentiometric method using an ion-selective electrode
PND F 14.1:2.230-06: Measurement of mass concentrations of acrylic acid nitrile and acetaldehyde in natural and waste waters using gas chromatography.
PND F 14.1:2:4.177-02: Quantitative chemical analysis of water. Methods for measuring the mass concentration of phenol in drinking, natural and waste water samples by gas-liquid chromatography
PND F 16.1.54-2008: Method for measuring the mass fraction of water-soluble mobile forms of fluorine (fluoride ions) in water extraction samples of the soil by direct potentiometry.
PND F 16.1:3.72-2012: Methods of measuring the mass fraction of nitrate ions in soil samples, waste from water treatment, wastewater treatment and water use by the potentiometric method
PND F 16.3.24-2000: Quantitative chemical analysis of soil. Methods for measuring the mass fractions of metals (iron, cadmium, aluminum, magnesium, manganese, copper, nickel, calcium, chromium, zinc) in samples of industrial waste (slags, sludge from metallurgical production) atomic absorption method
PND F T 14.1:2:3:4.10-2004: Toxicological methods of analysis. Methods for determining the toxicity of drinking, natural and waste waters, water extracts from the soil, sewage sludge and production and consumption waste by changing the optical density of the chlorella algae culture
R 50.2.090-2013: State system for ensuring the uniformity of measurements. Quantitative chemical analysis procedures. General requirements for development, certification and application
RD 52.18.750-2010: Mass concentration of phenols in waters. Measurement technique by high performance liquid chromatography using solid phase extraction. NGO "Typhoon"
RD 52.24.358-2019: Mass concentration of total iron and gross iron in waters. Measurement procedure with the photometric method with 1,10-phenanthroline
RD 52.24.360-2008: Mass concentration of fluoride in water. Measurement technique using potentiometric method with ion-indicating electrode.
RD 52.24.367-2010: Mass concentration of nitrates in waters. Methods for measuring by potentiometric method with ion-selective electrode
RD 52.24.373-2009: Mass concentration of zinc in waters. Measurement technique by the inversion voltamperometric method
RD 52.24.377-2008: The mass concentration of Aluminium, beryllium, vanadium, iron, cadmium, cobalt, manganese, copper, molybdenum, nickel, lead, silver, chromium and zinc in water. Methods of measurement by atomic absorption with a direct electrothermal atomization of samples.
RD 52.24.380-2017: Mass concentration of nitrate nitrogen in waters. Measurement technique by photometric method with Griess reagent after reduction in cadmium reducer
RD 52.24.381-2017: Mass concentration of nitrite nitrogen in water. Measurement procedure by photometric method with Griss reagent
RD 52.24.382-2019: Mass concentration of phosphate phosphorus in water. Photometric Measurement Method
RD 52.24.383-2018: Mass concentration of ammonia nitrogen in water. Measurement procedure by the photometric method in the form of indophenol blue
RD 52.24.387-2019: Mass concentration of total phosphorus and total phosphorus in waters. Measurement procedure by photometric method after oxidation with potassium persulfate
RD 52.24.389-2011: Mass concentration of boron in waters. The method of measurement using photometric method with azomethine-ASH
RD 52.24.390-2009: Mass concentration of xanthates in waters. Measurement Technique by Extraction-Photometric Method
RD 52.24.394-2012: Mass concentration of ammonium nitrogen in waters. Measurement technique by potentiometric method with ion-selective electrodes
RD 52.24.395-2017: Hardness of water. Measurement procedure by the titrimetric method with trilon B
RD 52.24.401-2018: Mass concentration of sulfates in water. Measurement procedure with lead nitrate titrimetric method
RD 52.24.402-2011: Mass concentration of chlorides in waters. Measurement Technique by Mercurimetric Method
RD 52.24.403-2018: Mass concentration of calcium ions in waters. Measurement technique using the trilon B titrimetric method
RD 52.24.405-2018: Mass concentration of sulfates in water. Measurement procedure by turbidimetric method
RD 52.24.406-2018: Mass concentration of sulfates in water. Measurement procedure by titrimetric method with barium chloride
RD 52.24.407-2017: Mass concentration of chlorides in water. Method of measurement by argentometric method
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RD 52.24.411-2009: Mass concentration of parathion-methyl, karbofos, dimethoate, fosalona in waters. The method of measurement by gas chromatography
RD 52.24.412-2009: Mass concentration of hexachlorobenzene, alpha-, beta- and gamma-HCCH, dicofol, dihydroheptachlor, 4, 4'-DDT, 4, 4'-DDE, 4, 4'-DDD, trifluralin in waters. The method of measurement by gas chromatography
RD 52.24.413-2011: Mass concentration of dalapon-sodium and sodium trichloroacetate in waters. The method of measurement by gas chromatography
RD 52.24.414-2012: Mass concentration of propanil and its metabolite 3, 4-dichloraniline in waters. The method of measurement by gas chromatography
RD 52.24.416-2010: Mass concentration of molybdenum in waters. Measurement technique by the inversion voltamperometric method
RD 52.24.417-2011: Mass fraction of organochlorine pesticides in bottom sediments. The method of measurement by gas chromatography
RD 52.24.419-2019: Mass concentration of dissolved oxygen in water. Methodology for measuring by iodometric method
RD 52.24.420-2006: Biochemical oxygen demand in waters. Measurement method using the bottle method
RD 52.24.420-2019: Biochemical oxygen consumption in waters. Measurement procedure by titrimetric and amperometric methods
RD 52.24.421-2012: Chemical oxygen consumption in waters. Measurement method titrimetric method
RD 52.24.423-2022: Mass concentration of methanol in waters. Methods of measurement by photometric method with chromotropic acid
RD 52.24.427-2013: Mass concentration of zinc, copper, iron, manganese and nickel in water. AAS measurement technique with atomization in flame
RD 52.24.428-2009: Mass concentration of total chromium and chromium (VI) in waters, measurement procedure using the inversion voltammetric method
RD 52.24.432-2018: Mass concentration of silicon in waters. Photometric measurement technique in the form of a blue (reduced) form of molybdosilicic acid
RD 52.24.433-2018: Mass concentration of silicon in waters. Measurement technique by photometric method in the form of a yellow form of molybdosilic acid
RD 52.24.435-2008: Mass concentration of copper in water. Methods of measuring the photometric method with 8, 8 '-dihinolildisulfidom
RD 52.24.436-2011: Mass concentration of cadmium in waters. Measurement technique photometric method with kadion
RD 52.24.438-2011: Mass concentration of MCPA and 2, 4-D in waters. Measurement method gas chromatography
RD 52.24.448-2009: Mass concentration of lead in waters. Methods for measuring by photometric method with hexaoxacycloazochrome
RD 52.24.450-2010: Mass concentration of hydrogen sulfide and sulfides in waters. Methods of measurement using photometric method with N, N-dimethyl-n-phenylenediamine
RD 52.24.452-2011: Mass concentration of dithiophosphates in waters. Measurement technique by extraction-photometric method
RD 52.24.459-2012: Mass concentration of eptam, molinata, triallate, thiobencarb in waters. Measurement method gas chromatography
RD 52.24.464-2011: Mass concentration of zinc in waters. Methods of measurement using densitometric method with reactive indicator paper
RD 52.24.465-2011: Mass concentration of copper in waters. Methods of measurement using densitometric method with reactive indicator paper
RD 52.24.466-2011: Mass concentration of total iron in waters. Measurement technique by densitometric method with reactive indicator paper
RD 52.24.468-2019: Mass concentration of suspended solids and solids in water. Gravimetric measurement procedure
RD 52.24.470-2014: Mass concentration of calcium and magnesium in waters. Measurement technique flame atomic absorption method
RD 52.24.472-2012: Mass concentration of hloridazona in waters. Measurement method gas chromatography
RD 52.24.473-2012: Mass concentration of volatile aromatic hydrocarbons in waters. Measurement technique by gas chromatography using equilibrium vapor analysis
RD 52.24.482-2012: Mass concentration of volatile chlorine substituted hydrocarbons in waters. Measurement technique by gas chromatography using equilibrium vapor analysis
RD 52.24.484-2012: Mass concentration of phenmedifam in the waters. Measurement method gas chromatography
RD 52.24.485-2012: Mass concentration of chlorpyrifos in waters. Measurement method gas chromatography
RD 52.24.486-2009: Mass concentration of ammonia and ammonium ions in waters. The method of measurement using the photometric method with Nessler's reagent
RD 52.24.487-2011: Mass concentration of phenol, alkylphenols and monochlorophenols in waters. Measurement method gas chromatography
RD 52.24.493-2020: Mass concentration of hydrocarbons and alkalinity of natural waters. Measurement procedure by titrimetric method
RD 52.24.495-2017: Hydrogen indicator of waters. Measurement procedure by potentiometric method
RD 52.24.504-2010: Mass concentration of fats in the waters. Measurement Technique by IR-Photometric Method
RD 52.24.505-2010: Mass fraction of oil components in bottom sediments. The method of measurement with the identification of their composition and origin of IR-photometric, luminescent and gas chromatographic methods
RD 52.24.506-2009: Mass concentration of acetone in waters. The method of measurement by gas chromatography
RD 52.24.507-2012: Mass concentration of di- and polychlorophenols in waters. Measurement method gas chromatographic method. Hydrochemical Institute (GHI)
RD 52.24.511-2013: Mass fraction of methane in bottom sediments. Measurement technique by gas chromatography using equilibrium vapor analysis
RD 52.24.512-2012: Volumetric concentration of methane in waters. Measurement technique by gas chromatography using equilibrium vapor analysis
RD 52.24.513-2014: Mass fraction of 4-7 nuclear polycyclic aromatic hydrocarbons in bottom sediments. Measurement technique by the luminescence method using thin-layer chromatography. Hydrochemical Institute (GHI)
RD 52.24.515-2019: Mass concentration of carbon dioxide in water. Measurement procedure by titrimetric and calculation methods
RD 52.24.519-2011: Mass concentration of cyanides and thiocyanates in waters. Methods of measurement by photometric method with barbituric (thiobarbituric) acid
RD 52.24.520-2011: Mass concentration of cyanides in waters. Methods for making measurements by the photometric method with nicotinamide
RD 52.24.521-2009: Mass concentration of iron (II) in waters. Methods for measuring by photometric method with 1, 10-phenanthroline. Hydrochemical Institute (GHI)
RD 52.24.522-2009: Mass concentration of total chromium in the waters. The method of measurement using photometric method with diphenylcarbazide
RD 52.24.523-2009: Mass concentration of nitrates in waters. Methods for measuring by photometric method with sulfanilamide and N- (1-naphthyl) ethylenediamine dihydrochloride after reduction in a cadmium reducer
RD 52.24.524-2009: Mass concentration of carbonates in waters. Titrimetric Measurement Technique
RD 52.24.525-2011: Mass fraction of sulfide sulfur in bottom sediments. The method of measurement using photometric method with N, N-dimethyl-n-phenylenediamine. Hydrochemical Institute (GHI)
RD 52.24.526-2012: Mass concentration of arsenic in waters. Measurement by atomic absorption method
RD 52.24.528-2012: Mass concentration of nitrates in waters. Measurement technique by photometric method with sulfanilamide and N- (1-naphthyl) ethylenediamine dihydrochloride after reduction with hydrazine sulfate
RD 52.24.529-2013: Mass concentration of polychlorophenols in waters. Measurement technique by gas chromatography after derivatization with monochloroacetic acid anhydride. Hydrochemical Institute (GHI)
RD 52.24.530-2016: Mass concentration of ammonia nitrogen in water. Procedure of measurement by photometric method in the form of derivatives of indophenol with salicylate
RD 52.24.531-2016: Chemical oxygen consumption in water. Procedure of measurements by titration method with sample mineralization in a thermal reactor
RD 52.24.532-2016: Mass concentration of total nitrogen in water. Measurement procedure by spectrophotometric method with sample digestion in thermal reactor
RD 52.24.533-2017: Mass concentration of fluorides in water. Photometric measurement method with lanthanum-alizarin complexone in the presence of acetone
RD 52.24.534-2019: Mass fraction of iron, manganese, copper, nickel and zinc in bottom sediments. Atomic absorption measurement method using microwave sample processing
RD 52.24.535-2019: Mass fraction of cadmium, cobalt, lead and chromium in bottom sediments. Atomic absorption measurement method using microwave sample processing
RD 52.24.536-2019: Mass concentration of iron, cadmium, cobalt, manganese, copper, nickel, lead, chromium and zinc in suspended solids of water. Atomic absorption measurement method using microwave sample processing
RD 52.24.539-2022: Mass concentration of polycyclic aromatic hydrocarbons in water. Measurement technique by high performance liquid chromatography with spectrofluorimetric detection
RD 52.44.588-2016: Mass concentration of organochlorine pesticides and the sum of polychlorbiphenyl isomers in air and precipitation samples. Method of measurement by gas-liquid chromatography
RD 52.44.589-2016: Mass concentration of priority components of polycyclic aromatic hydrocarbons in atmospheric air samples. Measurement technique by high performance liquid chromatography
RD 52.44.590-2016: Mass concentration of priority components of polycyclic aromatic hydrocarbons in samples of precipitation and surface water. Measurement technique by high performance liquid chromatography
RD 52.44.591-2015: Mass concentration of mercury in atmospheric air. Measurement procedure by cold vapour atomic absorption spectrometry'
RD 52.44.593-2015: Mass concentration of heavy metals in atmospheric air. Measurement technique by atomic absorption spectrometry with flameless atomization
RD 52.44.594-2016: Mass concentration of heavy metals in precipitation and surface waters. Measurement technique by atomic absorption spectrometry with flameless atomization
RD 52.44.816-2015: Mass concentration of methane and carbon dioxide in the surface layer of atmospheric air. Gas Chromatography Measurement Technique
RMG 76-2004: State system for ensuring the uniformity of measurements. Internal control of quantitative chemical analysis result's accuracy
RMG 76-2014: State system for ensuring the uniformity of measurements. Internal control of quantitative chemical analysis result's accuracy
ST RK GOST R 52991-2010: Water. Methods for determination of total and dissolved organic carbon
TSN 23-350-2004: Energy efficiency of residential and public buildings. Standards for energy consumption and heat protection. Vologodskaya Oblast
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