Determination of the content of toxic elements in food products and food raw materials. Autoclave Sample Preparation Technique
Определение содержания токсичных элементов в пищевых продуктах и продовольственном сырье. Методика автоклавной пробоподготовки
Status: Effective - Introduced for the first time
These guidelines provide a method for the mineralization of food samples and food raw materials using analytical autoclaves for the subsequent determination of the content of toxic elements (copper, zinc, lead, cadmium, arsenic, mercury, tin, nickel, iron, chromium, selenium, cobalt) using atomic spectrometry methods (atomic absorption spectrometry with atomization in a flame, in a graphite furnace and using the hydride generation technique, atomic emission spectrometry with inductively coupled plasma) and inversion-voltammetric method and are designed for laboratory research of food safety institutions of the state sanitary and epidemiological service of Russia.
Настоящие методические указания устанавливают способ минерализации проб пищевых продуктов и продовольственного сырья с использованием аналитических автоклавов для последующего определения содержания токсичных элементов (меди, цинка, свинца, кадмия, мышьяка, ртути, олова, никеля, железа, хрома, селена, кобальта) методами атомной спектрометрии (атомно-абсорбционной спектрометрией с атомизацией в пламени, в графитовой печи и с использованием техники генерации гидридов, атомно-эмиссионной спектрометрией с индуктивно-связанной плазмой) и инверсионно-вольтамперометрическим методом и предназначены для проведения лабораторных исследований безопасности пищевой продукции учреждениями госсанэпидслужбы России.
Format: Electronic (pdf/doc)
Page Count: 13
Approved: Chief State Sanitary Doctor of the Russian Federation,
The Product is Contained in the Following Classifiers:
Construction (Max) »
Regulatory documents of supervisory authorities »
Normative documents of State Committee for Sanitary and Epidemiological Supervision and Ministry of Health of Russian Federation »
Evidence base (TR CU, Technical Regulation of the Customs Union) »
021/2011 TR CU. About food safety »
Regulations and standards (to ТР ТС ТС 021/2011) »
SECTION I. TECHNICAL REGULATION »
V Testing and control »
4 Testing and control of products »
4.4 Testing and control of food products »
ISO classifier »
67 PRODUCTION OF FOOD »
67.050 General methods for food inspection and analysis »
The Document References:
GN 184.108.40.2066-98: Maximum Allowable Concentrations (PDK) of Hazardous Substances in Workplace Air. Hygienic Standards
GOST 10929-76: Reagents. Hydrogen peroxide. Specifications
GOST 11125-84: Super pure nitric acid. Specifications
GOST 12.1.004-91: Fire safety. General requirements
GOST 12.4.009-83: Fire-fighting equipment for protection of units. Basic types. Location and maintenance
GOST 1770-74: Laboratory volumetric glassware. Cylinders, beakers, measuring flasks, test tubes. General specifications
GOST 21400-75: Chemical and laboratory glass. Technical specifications. Test methods
GOST 24104-88: General purpose and reference laboratory balances
GOST 25336-82: Laboratory glassware and equipment. Basic parameters and dimensions
GOST 26929-94: Raw material and food-stuffs. Preparation of samples. Decomposition of organic matters for analysis of toxic elements
GOST 4461-77: Reagents. Nitric acid. Specifications
GOST 6709-72: Distilled water. Specifications
GOST 9147-80: Laboratory porcelain ware and apparatus. Specifications
The Document is Referenced By:
GOST R 51766-2001: Raw material and food-stuffs. Atomic absorption method for determination of arsenic
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GOST R 52819-2007: Canned goods from poultry meat for dietary (preventing) nutrition of toddlers. Specifications
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GOST R 55455-2013: Boiled-smoked meat sausages. Specifications
GOST R 55456-2013: Dry sausages. Specifications
GOST R 55477-2013: Meat cans from by-products. Specifications
GOST R 55485-2013: Fat products. Specifications
GOST R 55499-2013: Products of poultry meat. General specifications
GOST R 55574-2013: Meat pate for child food. Specifications
GOST R 55762-2013: Canned meat. Ham. Specifications
GOST R 55790-2013: Semi-prepared ground of poultry meat for children nutrition. Specifications
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GOST R 55796-2013: Pork smoked products. Specifications
GOST R 55797-2013: Canned poultry and rabbits meat for nutrition of pregnant women. Specifications
MUK 4.1.986-00: Measurement method for measuring the mass fraction of lead and cadmium in food products and food raw materials using electrothermal atomic absorption spectrometry
MUK 4.1.991-00: Measurement method for measuring the mass fraction of copper and zinc in food products and food raw materials by electrothermal atomic absorption spectrometry
PNST 280-2018: Russian system of quality. Comparative testing of pure natural honey
PNST 290-2018: Russian system of quality. Comparative testing of food chicken eggs
PNST 293-2018: Russian system of quality. Comparative testing of structured product from fish mince - crab sticks
SanPiN 220.127.116.118-01: Sanitary requirements to safety and nutritive value of food products
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