MUK 4.1.3489/1-17
МУК 4.1.3489/1-17
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Determination of residual amounts of fipronil and its metabolite fipronil sulfone in dry egg food products, eggs, meat and poultry by-products by capillary gas-liquid chromatography
Определение остаточных количеств фипронила и его метаболита фипронил-сульфона в продуктах яичных сухих пищевых, яйцах, мясе и субпродуктах птицы методом капиллярной газожидкостной хроматографии
Status: Effective - Introduced for the first time. Certificate of attestation MI No. ROSS RU.0001.310430
The guidelines establish the procedure for applying gas chromatography with mass-selective and electron-capture detectors to determine the mass concentration of fipronil and its metabolite fipronil sulfon in egg dry food products, eggs, meat and offal of poultry in the ranges of 0.002-0.05 mg
Методические указания устанавливают порядок применения метода газовой хроматографии с масс-селективным и электронозахватным детекторами для определения в продуктах яичных сухих пищевых, яйцах, мясе и субпродуктах птицы массовой концентрации фипронила и его метаболита фипронил-сульфона в диапазонах 0,002 - 0,05 мг/кг и 0,005 - 0,05 мг/кг
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Format: Electronic (pdf/doc)
Approved: Chief State Sanitary Doctor of the Russian Federation,
10/5/2017
SKU: RUSS372949
The Product is Contained in the Following Classifiers:
PromExpert »
SECTION I. TECHNICAL REGULATION »
V Testing and control »
4 Testing and control of products »
4.4 Testing and control of food products »
ISO classifier »
67 PRODUCTION OF FOOD »
67.050 General methods for food inspection and analysis »
The Document References:
GN 2.2.5.1313-03: Maximum allowable concentrations (MACs) of harmful substances in occupational air
GN 2.2.5.2308-07: Chemical factors of production environment. Tentative safe exposure levels (TSEL) for harmful substances in the air of the working zone
GOST 12.0.004-90: Organization of training for labor safety. General rules
GOST 12.1.004-91: Fire safety. General requirements
GOST 12.1.007-76: Noxious substances. Classification and general safety requirements
GOST 12.4.009-83: Fire-fighting equipment for protection of units. Basic types. Location and maintenance
GOST 1770-74: Laboratory volumetric glassware. Cylinders, beakers, measuring flasks, test tubes. General specifications
GOST 20490-75: Reagents. Potassium permanganate. Specifications
GOST 22300-76: Reagents. Ethyl acetate and butyl acetate. Specifications
GOST 23932-90: Laboratory glassware and equipment. General specifications
GOST 24861-91: Sterile hypodermic syringes for single use
GOST 25336-82: Laboratory glassware and equipment. Basic parameters and dimensions
GOST 2603-79: Reagents. Acetone. Specifications
GOST 28498-90: Liquid-in-glass thermometers
GOST 29227-91: Laboratory glassware. Graduated pipettes. Part 1. General requirements
GOST 30363-2013: Products egg dry and liquid food. Specification
GOST 31467-2012: Poultry meat, edible offal, and ready-to-cook poultry meat. Sampling methods and preparing of samples for examinations
GOST 31654-2012: Food chicken eggs. Specifications
GOST 4166-76: Reagents. Sodium sulphate. Specifications
GOST 4221-76: Reagents. Potassium carbonate. Specifications
GOST 4233-77: Reagents. Sodium chloride. Specifications
GOST 4523-77: Reagents. Magnesium sulphate 7-aqueous. Specifications
GOST 61-75: Reagents. Acetic acid. Specifications
GOST 9147-80: Laboratory porcelain ware and apparatus. Specifications
GOST 9737-93: Laboratory glassware. Interchangeable spherical ground joints
GOST OIML R 111-1-2009: State system for ensuring the uniformity of measurement. Weights of accuracy classes E1, E2, F1, F2, M1, M1-2, M2, M2-3 and M3. Part 1 Metrological and technical requirements.
GOST R 12.1.019-2009: Occupational safety standards system. Electrical safety. General requirements and nomenclature of kinds of protection
GOST R 52501-2005: Water for analytical laboratory use. Specifications
GOST R 53228-2008: Non-automatic weighing instruments. Part 1. Metrological and technical requirements. Tests
GOST R ISO 5725-1-2002: Accuracy (trueness and precision) of measurement methods and results. Part 1. General principles and definitions
GOST R ISO 5725-2-2002: Accuracy (trueness and precision) of measurement methods and results. Part 2. Basic method for the determination of repeatability and reproducibility of a standard measurement method
GOST R ISO 5725-3-2002: Accuracy (trueness and precision) of measurement methods and results. Part 3. Intermediate measures of the precision of a standard measurement method
GOST R ISO 5725-4-2002: Accuracy (trueness and precision) of measurement methods and results. Part 4. Basic methods for the determination of the trueness of a standard measurement method
GOST R ISO 5725-5-2002: Accuracy (trueness and precision) of measurement methods and results. Part 5. Alternative methods for the determination of the precision of a standard measurement method
GOST R ISO 5725-6-2002: Accuracy (trueness and precision) of measurement methods and results. Part 6. Use in practice of accuracy values
Order 116: Federal norms and rules in the field of industrial safety "Industrial safety rules for hazardous production facilities where equipment operating under excessive pressure is used"
Order 116: On the approval of the Federal norms and rules in the field of industrial safety "Industrial safety rules for hazardous production facilities using equipment operating under excessive pressure" (as amended on December 12, 2017) (canceled from 01.01.2021 on the basis of the Decree of the Government of the Russian Federation dated 06.08.2020 N 1192)
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