MUK 4.1.3562-19
МУК 4.1.3562-19
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Determination of residual amounts of oxathiapiproline in water, soil, potato tubers, onion turnips, tomato fruits and tomato juice, grapes and grape juice by high performance liquid chromatography with mass spectrometric detection
Определение остаточных количеств оксатиапипролина в воде, почве, клубнях картофеля, луке-репке, плодах томата и томатном соке, ягодах винограда и виноградном соке методом высокоэффективной жидкостной хроматографии с масс-спектрометрическим детектированием
Status: Effective
The guidelines establish the application of high performance liquid chromatography with mass spectrometric detection to determine the mass concentration of oxathiapiproline in water in the range of 0.005-0.050 mg / dm3 and in the soil in the range of 0.01-0.10 mg / kg, as well as the level of its residual amounts in potato tubers, onion turnips, tomato fruits and tomato juice, grapes and grape juice in the range of 0.01 - 0.10 mg / kg
Методические указания устанавливают порядок применения метода высокоэффективной жидкостной хроматографии с масс-спектрометрическим детектированием для определения массовых концентраций оксатиапипролина в воде в диапазоне 0,005 - 0,050 мг/дм3 и в почве в диапазоне 0,01 - 0,10 мг/кг, а также уровня его остаточных количеств в клубнях картофеля, луке-репке, плодах томата и томатном соке, ягодах винограда и виноградном соке в диапазоне 0,01 - 0,10 мг/кг
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Format: Electronic (pdf/doc)
Approved: Chief State Sanitary Doctor of the Russian Federation,
10/11/2019
SKU: RUSS378029
The Product is Contained in the Following Classifiers:
Construction (Max) »
Regulations »
Regulatory documents of supervisory authorities »
Normative documents of State Committee for Sanitary and Epidemiological Supervision and Ministry of Health of Russian Federation »
ISO classifier »
67 PRODUCTION OF FOOD »
67.080 Fruits. Vegetables »
67.080.01 Fruits, vegetables and their processed products in general »
The Document References:
GN 1.2.3539-18: Hygienic standards for pesticide content in environmental objects (the list)
GN 2.2.5.3532-18: Maximum permissible concentration (MPC) of harmful substances in the air of the working area
GOST 12.0.004-2015: Occupational safety standards system. Organization of training for labor safety. General principles
GOST 12.1.004-91: Fire safety. General requirements
GOST 12.1.007-76: Noxious substances. Classification and general safety requirements
GOST 12.1.019-2017: Occupational safety standards system. Electrical safety. General requirements and nomenclature of types of protection
GOST 12.4.009-83: Fire-fighting equipment for protection of units. Basic types. Location and maintenance
GOST 17.4.3.01-83: Nature protection. Soils. General requirements for sampling
GOST 1723-2015: Fresh onion for industrial processing. Specifications
GOST 1770-74: Laboratory volumetric glassware. Cylinders, beakers, measuring flasks, test tubes. General specifications
GOST 20490-75: Reagents. Potassium permanganate. Specifications
GOST 25336-82: Laboratory glassware and equipment. Basic parameters and dimensions
GOST 26832-86: Fresh potates for producing food products. Specifications
GOST 28168-89: Soils. Sampling
GOST 29227-91: Laboratory glassware. Graduated pipettes. Part 1. General requirements
GOST 31861-2012: Water. General requirements for sampling
GOST 32101-2013: Canned foods. Juice products. Juices from fresh fruit. General specifications
GOST 32786-2014: Fresh table grapes. Specifications
GOST 32876-2014: Juice products. Tomato juice. Specifications
GOST 34298-2017: Fresh tomatoes. Specifications
GOST 34306-2017: Fresh onion. Technical conditions
GOST 4166-76: Reagents. Sodium sulphate. Specifications
GOST 4201-79: Reagents. Sodium bicarbonate. Specifications
GOST 4233-77: Reagents. Sodium chloride. Specifications
GOST 5556-81: Medical absorbent cotton
GOST 5848-73: Reagents. Formic acid. Specifications
GOST 61-75: Reagents. Acetic acid. Specifications
GOST 6552-80: Reagents. Orthophosphoric acid. Specifications
GOST 6709-72: Distilled water. Specifications
GOST 6995-77: Reagents. Methanol-poison. Specifications
GOST 7176-2017: Potatoes food. Technical conditions
GOST 9147-80: Laboratory porcelain ware and apparatus. Specifications
GOST 9293-74: Gaseous and liquid nitrogen. Specifications
GOST ISO/IEC 17025-2019: General competency requirements for testing and calibration laboratories
GOST R 53228-2008: Non-automatic weighing instruments. Part 1. Metrological and technical requirements. Tests
GOST R 8.563-2009: State system for ensuring the uniformity of measurements. Procedures of measurements
GOST R ISO 5725-1-2002: Accuracy (trueness and precision) of measurement methods and results. Part 1. General principles and definitions
GOST R ISO 5725-2-2002: Accuracy (trueness and precision) of measurement methods and results. Part 2. Basic method for the determination of repeatability and reproducibility of a standard measurement method
GOST R ISO 5725-3-2002: Accuracy (trueness and precision) of measurement methods and results. Part 3. Intermediate measures of the precision of a standard measurement method
GOST R ISO 5725-4-2002: Accuracy (trueness and precision) of measurement methods and results. Part 4. Basic methods for the determination of the trueness of a standard measurement method
GOST R ISO 5725-5-2002: Accuracy (trueness and precision) of measurement methods and results. Part 5. Alternative methods for the determination of the precision of a standard measurement method
GOST R ISO 5725-6-2002: Accuracy (trueness and precision) of measurement methods and results. Part 6. Use in practice of accuracy values
RMG 61-2010: State system for ensuring the uniformity of measurements. Indicators of precision and accuracy of the quantitative chemical analysis techniques. Methods for evaluation
RMG 76-2014: State system for ensuring the uniformity of measurements. Internal control of quantitative chemical analysis result's accuracy
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