GOST 32587-2013
ГОСТ 32587-2013
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Grain and products of its processing, mixed feeds. Determination of ochratoxin A by high performance liquid chromatography
Зерно и продукты его переработки, комбикорма. Определение охратоксина А методом высокоэффективной жидкостной хроматографии
Status: Effective - Introduced for the first time. IUS 8-2014
This standard applies to grain and its products and establishes methods for determining the content of ochratoxin A using high performance liquid chromatography with fluorimetric detection using: - screening of samples and purification using column chromatography (method A) in food grains, wheat-based flour products , corn, barley, rye, oats and rice, mixed fodder and raw materials for their production on grain basis (cake, meal) in the range of measurements of the mass fraction of ochratoxin And from 0.0025 to 1.0 ppm; - cleaning by the method of solid phase extraction (method B) in the grain of cereals and flour in the range of measurements of the mass fraction of ochratoxin A more than 0.0004 million
Настоящий стандарт распространяется на зерно и продукты его переработки и устанавливает методы определения содержания охратоксина А с применением высокоэффективной жидкостной хроматографии с флуориметрическим детектированием с применением: - скрининга проб и очистки методом колоночной хроматографии (метод А) в продовольственном зерне, мукомольно-крупяных изделиях на основе пшеницы, кукурузы, ячменя, ржи, овса и риса, комбикормов и сырья для их производства на зерновой основе (жмых, шрот) в диапазоне измерений массовой доли охратоксина А от 0,0025 до 1,0 млн-1; - очистки методом твердофазной экстракции (метод Б) в зерне злаков и муке в диапазоне измерений массовой доли охратоксина А более 0,0004 млн
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Format: Electronic (pdf/doc)
Approved: Federal Agency for Technical Regulation and Metrology,
12/30/2013
SKU: RUSS72162
The Product is Contained in the Following Classifiers:
PromExpert »
SECTION I. TECHNICAL REGULATION »
V Testing and control »
4 Testing and control of products »
4.4 Testing and control of food products »
4.4.10 Products of feed industry »
PromExpert »
SECTION I. TECHNICAL REGULATION »
V Testing and control »
4 Testing and control of products »
4.3 Testing and control of agricultural and forestry products »
4.3.1 Crop products »
ISO classifier »
65 AGRICULTURE »
65.120 Animal feed »
National standards »
65 AGRICULTURE »
65.120 Animal feed »
ISO classifier »
67 PRODUCTION OF FOOD »
67.060 Cereals, legumes and their processed products »
National standards »
67 PRODUCTION OF FOOD »
67.060 Cereals, legumes and their processed products »
The Document References:
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GOST 12.1.007-76: Noxious substances. Classification and general safety requirements
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GOST 12.1.019-79: Occupational safety standards system. Electric safety. General requirements and nomenclature of kinds of protection
GOST 13586.3-83: Grain. Acceptance rules and sampling methods
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GOST ISO/IEC 17025-2009: General requirements for the competence of testing and calibration laboratories
GOST OIML R 76-1-2011: State system for ensuring the uniformity of measurements. Non-automatic weighing instruments. Part 1. Metrological and technical requirements. Tests
GOST R 52501-2005: Water for analytical laboratory use. Specifications
GOST R ISO 5725-2-2002: Accuracy (trueness and precision) of measurement methods and results. Part 2. Basic method for the determination of repeatability and reproducibility of a standard measurement method
GOST R ISO 5725-6-2002: Accuracy (trueness and precision) of measurement methods and results. Part 6. Use in practice of accuracy values
The Document is Referenced By:
Decision 236: On the list of international and regional (interstate) standards, and in their absence - national (state) standards, through the application of which on a voluntary basis compliance with the requirements of technical regulations of the Customs Union "On food safety" (TR CU 021/2011), and the list of international and regional (interstate) standards, and in their absence - national (state) standards, containing rules and methods of research (tests) and measurements, including rules from
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